Synthesis of dideoxyzearalane and related compounds

Details Synthesis of dideoxyzearalane and related compounds Synthesis of dideoxyzearalane and related compounds

1976-11-04

1978-05-09

Trousof, Natalie

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07D31300

Patent

active

040886581

ABSTRACT:
A method is disclosed for preparing dideoxyzearalane and related compounds which comprises reacting an appropriate hydroxy compound with an organic sulfonyl chloride to form a sulfonate ester derivative; recovering the sulfonate ester derivative; and catalytically hydrogenolyzing the sulfonate ester derivative to form the desired product.

REFERENCES:
patent: 3887583 (1975-06-01), Wehrmeister et al.
Wagner & Zook, Synthetic Org. Chem., p. 823.
March Advanced Org. Chem., p. 505.
Kenner et al. Chemical Abstracts 44, p. 565c, 1950.
Kenner et al. J. Chem. Soc., p. 406, 1950.

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