Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1979-02-15
1980-07-01
Sneed, Helen M. S.
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
C07F 504
Patent
active
042105994
ABSTRACT:
Improved synthesis of boroxarophenanthrenes, comprising the step of adding gaseous BCl.sub.3 to a liquid hydrocarbon slurry of 2-hydroxybiphenyl at a specified temperature. Known methods involve the reaction of BCl.sub.3 with the phenol at -70.degree. C., the reaction being carried out in methylene chloride.
REFERENCES:
patent: 3203928 (1965-08-01), Willcockson et al.
patent: 3287270 (1966-11-01), McCabe et al.
patent: 3397228 (1968-08-01), Brownstein
patent: 3417123 (1968-12-01), Offenhauer
patent: 3437596 (1969-04-01), McCabe
Barclay RaymondW.
Huggett Charles A.
Mobil Oil Corporation
Setliff Claude E.
Sneed Helen M. S.
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