Synthesis of boroxarophenanthrenes

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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C07F 504

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active

042105994

ABSTRACT:
Improved synthesis of boroxarophenanthrenes, comprising the step of adding gaseous BCl.sub.3 to a liquid hydrocarbon slurry of 2-hydroxybiphenyl at a specified temperature. Known methods involve the reaction of BCl.sub.3 with the phenol at -70.degree. C., the reaction being carried out in methylene chloride.

REFERENCES:
patent: 3203928 (1965-08-01), Willcockson et al.
patent: 3287270 (1966-11-01), McCabe et al.
patent: 3397228 (1968-08-01), Brownstein
patent: 3417123 (1968-12-01), Offenhauer
patent: 3437596 (1969-04-01), McCabe

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