Synthesis of bis(dichloroalumino)methane

Details Synthesis of bis(dichloroalumino)methane Synthesis of bis(dichloroalumino)methane

1987-11-05

1988-11-15

Shaver, Paul F.

Organic compounds -- part of the class 532-570 series

Organic compounds

Aluminum containing

C07F 506

Patent

active

047851252

ABSTRACT:
A process for the synthesis of bis(dichloroalumino)methane, with a lessened danger of runaway reaction, entails the gradual addition of methylene bromide to a heated mixture of aluminum and methylene chloride. An aluminum alkyl activator is also advantageously present as a scavenger for moisture and oxygen to prevent undesired oligomer formation.

REFERENCES:
patent: 3509189 (1970-04-01), Ort et al.
patent: 3509190 (1970-04-01), Ort et al.
patent: 3577450 (1971-05-01), Ort et al.
patent: 3700710 (1972-10-01), Mottus et al.
"J. Organomet. Chem.", (1973), pp. 47 to 52.

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