Synthesis of benzyl-metal compounds

Details Synthesis of benzyl-metal compounds Synthesis of benzyl-metal compounds

2006-06-27

2006-06-27

Nazario-Gonzalez, Porfirio (Department: 1621)

Organic compounds -- part of the class 532-570 series

Organic compounds

Heavy metal containing

C556S043000, C556S046000, C556S058000, C556S136000, C556S140000

Reexamination Certificate

active

07067686

ABSTRACT:
Disclosed are methods of producing di-, tri- or tetrabenzyl-metal compounds comprising combining a metal salt with a (benzyl)nMgX2-ncompound at from less than 30° C., wherein n is 1 or 2 and X is a monoanionic group; wherein the combining takes place in a diluent mixture comprising from 0 to 80% by volume of an ether diluent and a diluent selected from the group consisting of aromatic diluents, halogenated hydrocarbon diluents, and mixtures thereof. The methods are characterized by employing various mixtures of diluents, and in some cases, minimal to no ether diluent.

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