Synthesis of .alpha.-fluorocarbonyl compounds

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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260538R, 560 62, 560105, 560227, 562471, 562472, 562496, 2602393R, 2603435, 2603436, 2603974, 260326A, 546335, 549 70, 549 79, 562466, 562510, 560192, 560145, 568303, 568316, 568325, 568326, 568335, 568348, 568376, 568393, 568419, 568425, 568433, 568458, 568495, C07D24324

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042150442

ABSTRACT:
Process for preparing an organic compound of the formula R.sup.2 R.sup.2 CFC(O)R.sup.3, which process comprises contacting and reacting in a reaction mixture which includes an inert solvent, at a temperature of -40.degree. C. to -100.degree. C., ROF and ##STR1## R is polyfluoroperhaloalkyl of 1-6 carbon atoms or FOCF.sub.2 ; R.sup.1 is hydrocarbyl of 1-6 carbon atoms;

REFERENCES:
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House et al. "J. Org. Chem." vol. 34, No. 8, (1969) pp. 2324-2336.
Cady "Proc. Chem. Soc." (1960) pp. 133-138.
Sheppard "Organic Fluorine Chemistry" (Benjamin)(1969) pp. 124-127, 220-221, 230-231, 480-481.
Barton et al. "Chem. Comm." (1968), pp. 804-808.
Hoffman "Chemical Reviews" (1964) vol. 64, pp. 91-98.
Prager et al. "J. Am. Chem. Soc." vol. 87, No. 2, (1965) pp. 230-238.
Thompson "J. Am. Chem. Soc." vol. 89, No. 8, (1967) pp. 1811-1813.

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