Synthesis of a dithiol from 1-methyl-2-(2-hydroxyethylthio)-4-[1

Details Synthesis of a dithiol from 1-methyl-2-(2-hydroxyethylthio)-4-[1 Synthesis of a dithiol from 1-methyl-2-(2-hydroxyethylthio)-4-[1

1975-07-24

1977-03-22

Gotts, Lewis

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260609F, 260 47EC, C07C14926

Patent

active

040137244

ABSTRACT:
The synthesis of a new diol compound by the reaction of 2-mercaptoethanol and d,1-limonene to produce the diol 1-methyl-2-(2-hydroxyethylthio)-4[1-methyl-2-(2-hydroxyethylthio)ethyl]cyc lohexane. The diol can be used as an intermediate in a reaction with a thiourea for the synthesis of a new dithiol, 1-methyl-2-(2-mercaptoethylthio)-4-[1-methyl-2-(2-mercaptoethylthio)-ethyl ]cyclohexane.

REFERENCES:
patent: 2927946 (1960-03-01), Petty
patent: 3505166 (1970-04-01), Jones et al.
patent: 3652680 (1972-03-01), Buckholz
patent: 3729518 (1973-04-01), Mulheim et al.
patent: 3828100 (1974-08-01), Hickner et al.
patent: 3829501 (1974-08-01), Hickner
Amer. Chem. Soc., vol. 68, pp. 1871, 2103-2104 (1946).

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