Synthesis of 3-buten-1-ol, 3,4-dichlorobutan-1-ol and 3-chlorote

Details Synthesis of 3-buten-1-ol, 3,4-dichlorobutan-1-ol and 3-chlorote Synthesis of 3-buten-1-ol, 3,4-dichlorobutan-1-ol and 3-chlorote

1980-07-28

1981-09-08

Raymond, Richard

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

568848, 568879, C07C 2916, C07C 2962, C07D30718

Patent

active

042883741

ABSTRACT:
Tetrahydrofuran is prepared by reacting propylene and aqueous formaldehyde stabilized with alcohol in the presence of silica sand to form 3-buten-1-ol and chlorinating the 3-buten-1-ol in the presence of Group IA or IIA chloride to form 3,4-dichlorobutan-1-ol which is then treated with a Group IA or IIA base to form 3-chlorotetrahydrofuran which is then hydrogenated to form tetrahydrofuran.

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