Surfactant assisted nanomaterial generation process

Compositions – Solids with solution or dispersion aids

Reexamination Certificate

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C264S004100, C264S005000

Reexamination Certificate

active

10193363

ABSTRACT:
A process for the preparation of nanoscale particulate material is described comprising: (i) combining one or more functional material to be precipitated as nanoscale particles and one or more surface active material in a compressed CO2phase with a density of at least 0.1 g/cc, where the functional material is substantially insoluble in the compressed CO2in the absence of the surfactant, the surfactant comprises a compressed CO2-philic portion and a functional material-philic portion, and the compressed CO2phase, functional material and surfactant interact to form an aggregated system having a continuous compressed CO2phase and a plurality of aggregates comprising surfactant and functional material molecules of average diameter less than 10 nanometers dispersed therein; and (ii) rapidly depressurizing the compressed CO2phase thereby precipitating the dispersed functional and surfactant materials in the form of composite particles of average diameter from 0.5 to less than 10 nanometers.

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