Optics: measuring and testing – Standard – Surface standard
Reexamination Certificate
1999-11-12
2001-12-25
Pham, Hoa Q. (Department: 2877)
Optics: measuring and testing
Standard
Surface standard
Reexamination Certificate
active
06333785
ABSTRACT:
BACKGROUND OF THE INVENTION
1. Field of the Invention
The invention relates to a reproducible standard for calibrating and checking the bright field channel of a surface inspection device which is used for examinations of a smooth surface of a specimen. The invention also relates to a method for making the standard
2. The Prior Art
Smooth surfaces of a specimen, for example the sides of semiconductor wafers, are customarily examined using surface inspection devices, the surface to be examined being automatically scanned using a laser beam. Defects on the surface of the specimen, in particular raised and lowered portions of materials, and also foreign particles, can be identified and quantified by detecting and evaluating the light scattered by the surface of the specimen. For measurements in the dark field channel of the surface inspection device, that is to say for measurements of the scattered light produced non-specularly when the laser beam strikes, internationally recognized standards are available, using which the dark field channel of the surface inspection device can be calibrated and checked. Such a standard consists, for example, of a polished semiconductor wafer, on one of whose sides a particular number of microspheres with particular average size and size distribution are deposited.
The microspheres represent only a rough approximation of the defects which are actually to be found on smooth surfaces. Furthermore, especially defects which, over a comparatively large lateral extent, span only small height differences, are not detected in the dark field channel. They can, however, be picked up in the bright field channel of the surface inspection device, that is to say by measuring the laser light reflected specularly from the surface of the specimen. They are picked up customarily by measuring intensity losses of the laser beam reflected in the specular direction or by measuring the differential interference contrast (“Normaski contrast”). However, there is currently no reliable standard with which the bright field channel of the surface inspection device can be checked and calibrated. Standards which are based on substrates that have microspheres applied to them are found to be unsatisfactory for examinations in the bright field channel. A bright field standard of this kind must have comparatively large microspheres applied to it. Since the adhesion of microspheres to a substrate decreases as the sphere diameter increases, it is difficult to work with the standard. Furthermore, such a standard is not cleanable. It has also been found inappropriate to use known step-height standards as standards for measurements in the bright field channel. This is because, when such standards are used, no evidence of edge gradients of defects is encountered, so that realistic defect characterization is not possible.
SUMMARY OF THE INVENTION
The present invention achieves the object of providing a standard which is suitable for calibrating and checking the bright field channel of a surface inspection device.
The invention relates to a reproducible standard for calibrating and checking the bright field channel of a surface inspection device which is used for examinations of a smooth surface of a specimen, and to a method for making the standard, a microstructure being produced on a surface of a substrate provided as a standard, which is characterized in that the microstructure undergoes a smoothing treatment.
The standard is distinguished, in particular, in that defects found on the smooth surface of a specimen which are detectable in the bright field channel are realistically replicated by microstructures applied to the standard. The standard can therefore also advantageously be used for statistical process control (SPC) purposes. Furthermore, the standard can be reproduced with high accuracy. The bright field channel signal that can be detected when carrying out measurement on the standard can be directly attributed to a specific defect geometry. The standard can moreover be cleaned without problem. Lastly, with the aid of the standard, it is also possible to establish differences in sensitivity of the bright field channel with respect to a surface to be tested.
In order to make the standard, a substrate is needed which has at least one planar surface on which a microstructure can be formed. Preferred substrates are semiconductor wafers, in particular monocrystalline semiconductor wafers of silicon, which have at least one prepolished or mirror-polished side. These semiconductor wafers may also be coated, for example with an oxide layer, a nitride layer or with an epitaxial layer. In a first step of the method, the planar surface of the substrate, or a part of this surface, is structured. Microstructures are produced on the surface using methods which are known per se. Particularly preferred methods are lithographic methods, for example photolithography, ion beam. (focussed ion beam) lithography and electron beam lithography, as well as structuring methods using etching (micromachining) and plasma etching. Of course, combinations of the said methods may also be used for structuring the surface of the substrate.
Preferred microstructures are patterns of regularly repeating geometrical objects, the extent of an object being preferably from 1 &mgr;m 400 &mgr;m in width and lengths and from 1 nm to 1 &mgr;m in height. The object may be formed as raised or lowered parts, which protrude from the substrate plane and cut into the substrate, respectively. Examples of such objects include columnar raised or lowered parts. In contrast to microspheres deposited on the substrate surface, the objects form an integral unit with the substrate.
In principle, signals in the bright field channel of a surface inspection device can be recorded just with substrates structured in this way. However, the geometry of the objects still differs substantially from the geometry of the defects which are customarily found on the specimens to be examined. In particular, such objects have high edge gradients. In order to obtain a reliable standard for calibrating and checking the bright field channel, it is therefore proposed to carry out a smoothing treatment on the structured surface of the substrate. By such a treatment, in particular, edges are removed and the objects are altered in such a way that their appearance is modelled on that of the defects to be found on the surface of specimens.
The smoothing treatment is preferably carried out by polishing, plasma etching, etching with a non-preferential. etch or by a combination of the said methods.
The bright field channel of a surface inspection device is regularly calibrated and checked using standards made in the described way. Defects, which are detectable in the bright field channel, on smooth surfaces of specimens can then be quantitatively determined using the surface inspection device in automatically performed serial examinations, and assigned in terms of appearance and size to a particular type of defect.
Specimens for automatic serial examinations are, in particular, semiconductor wafers, for, example monocrystalline silicon wafers, coated semiconductor wafers, optical displays (flat panel displays) as well as electronic and optical storage media (discs, compact discs, hard disks).
REFERENCES:
patent: 4386850 (1983-06-01), Leahy
patent: 5383018 (1995-01-01), Sadjadi
patent: 5599464 (1997-02-01), Laind et al.
patent: 6130016 (2000-10-01), Kent
patent: 0 180 756 (1986-05-01), None
patent: WO92/07248 (1992-04-01), None
Patent Abstracts of Japan, vol. 018, No. 399 (P-1776) Jul, 26, 1994 & JP 06 117845 A (Advantest (Corp.), Apr. 28, 1994.
Gerber Hans-Adolf
Graf Dieter
Kerschreiter Robert
Luger Anton
Schmolke Rüdiger
Collard & Roe P.C.
Pham Hoa Q.
Wacker Siltronic Gesellschaft fur Halbleitermaterialien AG
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