Stable solid 2-octynyl adenosine and process for producing the s

Details Stable solid 2-octynyl adenosine and process for producing the s Stable solid 2-octynyl adenosine and process for producing the s

1992-02-11

1999-08-17

Knode, Marian C

Organic compounds -- part of the class 532-570 series

Organic compounds

Carbohydrates or derivatives

536 276, 536 2761, 536 2762, 514 26, C07H 19167

Patent

active

059395435

ABSTRACT:
The present invention provides two kinds of solid 2-octynyl adenosine products with novel properties which are stabilized with respect to temperature or temperature and humidity, one being solid 2-octynyl adenosine having a moisture content of not more than 3%, and the other being solid 2-octynyl adenosine deposited from an anhydrous alcoholic solution or hydrous alcoholic solution of 2-octynyl adenosine, said hydrous alcoholic solution having a water content of less than 1%.

REFERENCES:
patent: 4956345 (1990-09-01), Miyasaka et al.
"Aldrich Catalog/Handbook of Fine Chemicals," Aldrich Chemical Company, Milwaukee, WI, 1984-1985, p. 1358.
Matsuda et al. (I), Nucl. Acids Res. Symp. Ser., 16, 97-100 (1985).
Matsuda et al.(II), Nucl. Acids Res. Symp. Ser., 12, 5-8 (1983).
Matsuda et al.(III), Chem. Pharm Bull., 33(4), 1766-1769 (1985).
Weygand et al., "Preparative Organic Chemistry," Hilgetag et al. eds., John Wiley and Sons, New York, 1972, see pp. 1096-1098, 1111-1121, 1127.

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