Spray-drying process

Cleaning compositions for solid surfaces – auxiliary compositions – Cleaning compositions or processes of preparing – Heterogeneous arrangement

Reexamination Certificate

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Details

C510S452000

Reexamination Certificate

active

07811980

ABSTRACT:
The present invention relates to a process for preparing a spray-dried powder comprising (i) anionic detersive surfactant; (ii) from 0 wt % to 10 wt % zeolite builder; (iii) from 0 wt % to 10 wt % phosphate builder; and (iv) optionally from 0 wt % to 15 wt % silicate salt; wherein the process comprises the steps of: (a) forming an alkaline slurry in a mixer, the slurry comprising: (v) from 0 wt % to 15 wt % anionic detersive surfactant; (vi) from 0 wt % to 35 wt % water; and (b) transferring the alkaline slurry from the mixer through at least one pump to a spray pressure nozzle; (c) contacting an acid anionic detersive surfactant precursor to the alkaline slurry after the mixer and before the spray pressure nozzle to form a mixture; (d) spraying the mixture through the spray pressure nozzle into a spray-drying tower; (e) spray-drying the mixture to form a spray-dried powder; and (f) optionally, contacting an alkalinity source with the alkaline slurry and/or the acid anionic detersive surfactant precursor, and/or the mixture.

REFERENCES:
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patent: 6528474 (2003-03-01), Gonzalez et al.
patent: 7078373 (2006-07-01), Burrows et al.
patent: 2003/0203832 (2003-10-01), Boucher et al.
patent: 2005/0101503 (2005-05-01), Caldwell et al.
patent: 2006/0035802 (2006-02-01), Brooker et al.
patent: 2006/0035803 (2006-02-01), Mort et al.
patent: 2007/0037726 (2007-02-01), Brooker et al.
patent: 273688 (1991-09-01), None
patent: WO 96/03488 (1996-02-01), None
PCT International Search Report, dated Feb. 20, 2009—3 pgs, (for EP08159025).

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