Solvents for NMR spectroscopy

Chemistry: physical processes – Physical processes – Crystallization

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23230M, 2603406, 2604651, 260488R, 260541, 260551P, 260553R, 260561R, 260593R, 260607D, 260614R, 260632R, 260644, 260654R, 260668R, 324 5A, C07C 2900, C07C 5308, G01N 2700, G01N 3300

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active

039544109

ABSTRACT:
Organic solvents containing less than 0.2 atom percent of .sup.13 C and which preferably are at least partially deuterated are produced from .sup.13 C-depleted gaseous carbon compounds and are advantageously employed as solvents for .sup.13 C NMR spectroscopy.

REFERENCES:
patent: 3439260 (1969-04-01), Bene
patent: 3525036 (1970-08-01), Bene
patent: 3700410 (1972-10-01), Sievers
patent: 3702831 (1972-11-01), Chiarelli et al.
patent: 3730687 (1973-05-01), Rondeau
patent: 3756779 (1973-09-01), Rondeau et al.
patent: 3846333 (1974-11-01), Sievers
J. A. Pople et al., High-resolution Nuclear Magentic Resonance, p. 306-312 (1959).

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