Solvent process for hydrolyzing 5-isothiocyano-5,6-dihydrodicycl

Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing

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C07C 8300

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active

042592607

ABSTRACT:
5-Isothiocyano-5,6-dihydro-dicyclopentadiene is hydrolyzed with caustic to 5-amino-5,6-dihydro-dicyclopentadiene in a reaction medium comprising a polar organic liquid which is inert under the reaction conditions and which at least partially dissolves the reactants and products.

REFERENCES:
patent: 3088977 (1963-05-01), Segel
patent: 3150183 (1964-09-01), Buntin
patent: 3154579 (1964-10-01), Flanagan
patent: 3238251 (1966-03-01), Williams
patent: 3304167 (1967-02-01), Buntin et al.
"J. Org. Chem.", 34, pp. 616-624, 1969.

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