Solvent dried polysaccharide sponges

Drug – bio-affecting and body treating compositions – Designated organic active ingredient containing – Carbohydrate doai

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424443, 514 54, 514 55, 514 56, 514 57, 514 58, 514 59, 514 60, 536123, 5361231, A61K 31715, A61F 1300

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active

058889876

ABSTRACT:
The invention provides a method of preparing water-insoluble polysaccharide sponges, and sponges obtained by means of the method. The method comprises: (a) providing an aqueous solution of a soluble polysaccharide; (b) freezing the solution; (c) treating the frozen solution with a water-miscible organic solvent such as isopropanol to effect solvent exchange for the water in the frozen solution; and (d) drying the resulting polysaccharide material. The organic solvent contains a cross-linking agent such as calcium chloride to render the polysaccharide water-insoluble in the solvent-exchange step (c). The resulting materials are more conformable and less friable than freeze-dried polysaccharide sponges.

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patent: 5660857 (1997-08-01), Haynes et al.
Oungbho et al. Int. J. Pharm., vol. 156(2):229-237, (1997). Abstract Only.
Dumitriu et al. "Hydrogel Based Polysaccharides" From Polysaccharides in Medicinal Applications, ed. by Dumitriu, Severian; Marcel Dekker, pp. 125-171, (1996).
Dumitriu et al. "Hydrogels as Support For Drug Delivery Systems", Ibid. (pp. 705-717).
UK Search Report Application No. GB 9622394.6, 16 Jan. 1997, JJM-262.

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