Mineral oils: processes and products – Paraffin wax; treatment or recovery – Separation of paraffin from oil
Patent
1977-07-05
1978-09-19
Levine, Herbert
Mineral oils: processes and products
Paraffin wax; treatment or recovery
Separation of paraffin from oil
208 37, C10G 4308
Patent
active
041152450
ABSTRACT:
A solvent dewaxing process wherein an intermediate range waxy distillate oil, heated for dissolving all wax therein, is mixed with about 1-4 volumes dewaxing solvent having a temperature in the range of 60.degree.-80.degree. F for forming an oil-solvent mixture having a temperature below depressed cloud point. The oil-solvent mixture is subsequently cooled at 1.degree.-8.degree. F/min to a selected separation temperature for precipitating wax and forming a first wax/oil/solvent mixture. Additional solvent, at about the separation temperature, is mixed with first wax/oil/solvent mixture in an amount equivalent to about 1-2 volumes of waxy oil charge for precipitating additional wax and forming a second wax/oil/sovent mixture. Precipitated wax is separated, at said separation temperature from said second wax/oil/solvent mixture.
REFERENCES:
patent: 2410483 (1946-11-01), Dons et al.
patent: 3720599 (1973-03-01), Gould
patent: 3764517 (1973-10-01), Bodemuller
Chen et al., "Chemical Engineering", Mar. 19, 1973, pp. 105 to 111.
Harrison Charles W.
Watts Leonard R.
Levine Herbert
May, Jr. Douglas H.
Ries Carl G.
Texaco Inc.
Whaley Thomas H.
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