Solution doping of porous preforms

Glass manufacturing – Processes – Forming product or preform from molten glass

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65 182, 65901, 65 603, 65 3013, 264 15, 501 37, C03C 2502

Patent

active

051511177

ABSTRACT:
Disclosed is a method of forming a doped glass body. The glass body is formed by adding a dopant to a glass preform, at least part of which has interconnective pores. The porous preform is immersed in a solution of a salt of the dopant dissolved in an organic solvent having no OH groups. The solvent is removed, and the porous glass preform is heat treated to consolidate it into a non-porous glassy body containing the dopant dispersed throughout at least a portion of the body. An OH-free solvent is selected because of its beneficial effect on the preform during the drying step. Whereas OH-containing solvents such as water and alcohol caused cracking and/or flaking of the outer surface of the porous preform following the drying step, an undamaged surface is formed by the present invention.

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patent: 4414012 (1983-11-01), Suto et al.
patent: 5047076 (1991-09-01), Cognolato et al.

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