Solidification of crystalline silicon from reusable crucible...

Single-crystal – oriented-crystal – and epitaxy growth processes; – Forming from vapor or gaseous state – With decomposition of a precursor

Reexamination Certificate

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C117S097000, C427S133000, C427S154000, C427S372200, C427S421100, C427S428100, C428S213000

Reexamination Certificate

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07540919

ABSTRACT:
A process for making silicon ingots using a multi-part, reusable, graphite crucible of at least two mold pieces configured for assembly into an open top mold having an interior surface functional as a mold cavity for receiving molten silicon; removing or reducing a prior applied release coating from the interior surface until a uniformly smooth finish is achieved; coating the interior surface with a first layer of release coating comprising silicon nitride; coating the interior surface with a second layer of release coat comprising silica suspended in water; coating the interior surface with a third layer of release coat comprising silicon nitride; curing the release coat on said crucible; casting a silicon ingot in the crucible; and then repeating the prior steps multiple times.

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patent: 6083625 (2000-07-01), Fiel et al.
patent: 6165425 (2000-12-01), Lange et al.
patent: 6426133 (2002-07-01), Kondo et al.
patent: 6479108 (2002-11-01), Hariharan et al.
patent: 6491971 (2002-12-01), Costantini et al.
“A Reusable Mold in Directional Solidification for Silicon Solar Cells”, Solar Energy Materials, vol. 9, (1983), pp. 337-345, Saito, et al.
PCT Search Report dated Aug. 11, 2007 of Patent Application No. PCT/US06/12017 filed Mar. 31, 2006.

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