Solid phase synthesis reaction vessel and method of using the sa

Details Solid phase synthesis reaction vessel and method of using the sa Solid phase synthesis reaction vessel and method of using the sa

1997-09-04

1998-12-22

McMahon, Timothy

Chemical apparatus and process disinfecting, deodorizing, preser

Chemical reactor

Organic polymerization

422 50, 422 681, 422134, 422138, 435 87, 435 88, 525 50, 525 5411, 530333, 530334, C08F 200

Patent

active

058514945

ABSTRACT:
A solid phase synthesis reaction vessel includes a vessel with a first inlet, a second inlet, and an outlet. A first stopcock is disposed within the first inlet and a second stopcock is disposed within the outlet. Solid phase material is prevented from escaping the reaction vessel via the outlet while allowing fluid to flow through the outlet by a frit. In one embodiment, the reaction vessel includes an outer hollow shell surrounding the vessel to allow cooling or heating fluid to flow therein for controlling the temperature in the interior reaction volume. The solid phase synthesis reaction vessel provides for the independent opening and closing of each of the inlets and outlet to provide for various ways of draining the vessel, varying the conditions within the vessel, and/or adding additional materials into the vessel.

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Stewart, J. M. & Young, J. D. ; (1984) Solid Phase Peptide Synthesis (Pierce Chem. Co., Rockford, IL) 2nd Ed., pp.125-139.

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