Solid phase synthesis of protected peptides

Details Solid phase synthesis of protected peptides Solid phase synthesis of protected peptides

1975-05-07

1977-12-13

Phillips, Delbert R.

Chemistry: electrical and wave energy

Processes and products

Processes of treating materials by wave energy

204 1R, 2041601, 260 8, 260 78A, 2601125R, 526 52, 260 6, 260 7, C08L 8100

Patent

active

040627462

ABSTRACT:
The invention is addressed to the preparation of 3-nitro-4-bromomethyl benzoic acid, as a new compound from which 3-nitro-4-bromomethyl benzoyl amide polystyrene resin can be prepared for solid synthesis of protected peptide acids and amides and separation thereof without cleavage of acid labile protecting groups or decomposition of aromatic acid groups and from which purified polypeptides can be formed.

REFERENCES:
patent: 3573253 (1971-03-01), Gray
patent: 3645996 (1972-02-01), Southard
patent: 3700609 (1972-10-01), Tregear et al.
patent: 3775378 (1973-11-01), Dahimans et al.
patent: 3784523 (1974-01-01), Loffet
patent: 3814732 (1974-06-01), Wang
Rich et al., Chem. Comm., 1973, 610-611.
Barltrop et al., Chem. Comm., 1966, 822-823.

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