Solid phase microextraction fiber cleaning and conditioning...

Drying and gas or vapor contact with solids – Apparatus – Houses – kilns – and containers

Reexamination Certificate

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C034S219000, C034S234000, C034S241000, C034S443000

Reexamination Certificate

active

07047661

ABSTRACT:
A SPME-fiber cleaning and conditioning apparatus and method having an elongated heating chamber with first and second opposite ends. The first end is capable of insertably receiving a SPME fiber portion of a SPME device, and the second end is a fluid outlet. A heater is provided for heating the chamber and heat-treating an inserted SPME fiber. Contaminants and other particles are agitated, desorbed and purged from the inserted SPME fiber by flowing a fluid through the chamber from the first end to the second end, away from the SPME device. Additionally, turbulence may be produced in the flow at a location adjacent the first end, to enhance agitation, desorption, and purging. A holder may also be provided extending from the first end for supporting the SPME device in a substantially horizontal orientation when the SPME fiber is positioned in the chamber.

REFERENCES:
patent: 5691206 (1997-11-01), Pawliszyn
patent: 6537827 (2003-03-01), Pawliszyn
patent: 6623545 (2003-09-01), Thordarson et al.
patent: 2002/0182746 (2002-12-01), Mester et al.
Koziel, Jacek A. et al, Fiber Conditioners for Solid Phase Microextraction: Design, Testing and Application, Short Communications.

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