Soap fiber extraction process

Electrolysis: processes – compositions used therein – and methods – Electrolytic material treatment – Organic

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205696, 204450, 204513, 204514, 204553, 252 41, C10M17700, G01N 1100

Patent

active

057025886

ABSTRACT:
A method of separating soap fibers from the liquid phase component of grease to prepare the fibers for microscopic analysis includes the steps of admixing a sample of the grease with a solvent to remove the liquid phase component from the fibers and provide a final liquid product having the fibers in suspension therein, contacting the final product with a pair of spaced electrodes, applying a direct voltage across the electrodes to charge the same positive and negative respectively, and withdrawing for analysis a small quantity of the final product from a region thereof proximate the negative electrode after the voltage has been applied for a predetermined energization period. The withdrawn quantity may be deposited on a polished carbon stub and further prepared for analysis by a scanning electron microscope.

REFERENCES:
patent: 4444669 (1984-04-01), Wittse, Jr. et al.
patent: 4728403 (1988-03-01), Renzler
patent: 5583284 (1996-12-01), Martin et al.

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