Simplified synthesis of dialkylgold(III) .beta.-diketonates

Details Simplified synthesis of dialkylgold(III) .beta.-diketonates Simplified synthesis of dialkylgold(III) .beta.-diketonates

1990-05-01

1991-06-11

Prescott, Arthur C.

Organic compounds -- part of the class 532-570 series

Organic compounds

Heavy metal containing

556110, 556112, 556113, C07F 112

Patent

active

050233602

ABSTRACT:
Dialkyl gold(III) .beta.-diketonates are synthesized in a two-step, one-pot process using a gold trihalide, an alkyl lithium compound and a .beta.-diketone.

REFERENCES:
Gilman, H. and Woods, L. A. "Trimethylgold," Journal of American Chemical Society; vol. 70, pp. 550-552 (1948).
Chemical Abstracts, vol. 93, No. 11; Sep. 15, 1980, p. 747, Abstract No. 114651p.
Zharkova, G. I.; Igremenov, I. K.; Zemskov, S. V., "Chelates of dimethylgold (III) with p-diketones."
Koord Khim (Sov J Coord Chem.) 6th 1980 pages 720-23.
Zharkova et al. "Chelates of Dimethylgold(III) with beta-Diketones" in Russian J. Chem. Soc. 762-67 (1939) Brain et al. "The Organic Compounds of Gold" Part VII; Methyl and Ethyl Compounds.
J. A. Chem. Soc. 99, pp. 3695-3703 (1977). Komiya et al. "Reversible Linkage by Isomerisms of beta-Dikenato Ligands, Oxygen-Bonded and Carbon-Bonded Structures in Gold(III) Acetylacetonate Complexes Induced by Phosphines".

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