Silylation process

Details Silylation process Silylation process

1981-07-06

1983-08-23

Rizzo, Nicholas S.

Organic compounds -- part of the class 532-570 series

Organic compounds

Nitrogen attached directly or indirectly to the purine ring...

2602452R, 2602391, 544 26, 544 27, 548136, 548251, 548255, 548263, 548337, C07D50104

Patent

active

044005091

ABSTRACT:
An improved process for the trimethylsilylation of organic compounds with at least one active hydrogen atom with hexamethyldisilazane, the improvement comprising effecting the reaction in the presence of 0.001 to 10 mole percent of a catalyst of the formula

REFERENCES:
Harpp et al., JACS vol. 100, p. 1222 (1978).
Evans, JACS vol. 99, 5009 (1977).
Cephalosporins and Pencillins pp. 179-180 (1972) edited by E. Flynn (Academic Press, N.Y.).

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