Silicone resin coating for electronic components

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From silicon reactant having at least one...

Reexamination Certificate

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C528S032000, C528S043000

Reexamination Certificate

active

07666969

ABSTRACT:
One-component, H-siloxane-containing addition-crosslinkable silicone resins, are prepared by charging a reactor with water and a solvent mixture of at least one aromatic solvent and at least one alkyl ester, adding a chlorosilane mixture containing an Si—H functional silane and a silane bearing an unsaturated hydrosilylatable group with stirring, the temperature not being above 50° C., separating an aqueous phase comprising a one-component, H-siloxane-containing addition-crosslinkable silicone resin, and washing the phase comprising the one-component, H-siloxane-containing addition-crosslinkable silicone resin in at least two washing steps to reduce residual HCl content, a final washing carried out using a 0.01%-1.0% strength aqueous solution of a base with a pH between 7.00-8.50, at a temperature of 20-50° C.

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Kopylov et al., “Features of Influence of HC1 on Hydrolytic Copolycondensation of Bifunctional Organochlorosilanes with Trimethylchlorosilane”, Journal of General Chemistry USSR, Consultants Bureau, New York, NY, US, vol. 61, No. 6, Jun. 1, 1991, pp. 1257-1261.
English Abstract Corresponding to DE 102 12 119 A1.
English Abstract Corresponding to JP 2004-140220 A.
Noll: “Chemie Und Technologie Der Silicone”, 2nd Edition 1968, p. 574, Chapter 12.1.2.
English Version of Noll: “Chemic Und Technologie Der Silicone”, i.e., “Chemistry and Technology of Silicones”, 2nd Edition 1968, p. 574, Chapter 12.1.2.

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