Compositions: ceramic – Ceramic compositions – Carbide or oxycarbide containing
Patent
1993-03-05
1994-01-11
Bell, Mark L.
Compositions: ceramic
Ceramic compositions
Carbide or oxycarbide containing
501 95, C04B 3556
Patent
active
052781100
ABSTRACT:
A method of preparing preceramic SiC fibers having a very low oxygen content by forming fibers from a solution of a polycarbosilane and a vinylic sic precursor in a mutual volatile solvent, heating fibers in an oxygen-free inert s atmosphere to effect a cross-linking reaction therebetween. Also disclosed is a method of preparing SiC fibers having superior high temperature properties and a very low oxygen content comprising beating the above-described cross-linked preceramic fibers in an inert atmosphere substantially free of oxygen for a time and at a temperature sufficient to pyrolyze the cross-linked fibers to SiC fibers. The disclosure also describes the novel fibers produced by the above-described methods.
REFERENCES:
patent: 4100233 (1978-07-01), Vajima et al.
patent: 5063107 (1991-11-01), Birchall et al.
patent: 5071600 (1991-12-01), Deleeuw et al.
patent: 5139871 (1992-08-01), Wallace et al.
Batich Christopher D.
Toreki William
Bell Mark L.
Marcantoni Paul
University of Florida
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