Separation system and process

Liquid purification or separation – Processes – Chromatography

Reexamination Certificate

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C210S198200, C127S046200

Reexamination Certificate

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07060188

ABSTRACT:
The invention relates to a system and a process for fractionating a solution into two or more fractions. The system of the invention comprises at least two compartments having a diameter of at least about one meter and including a uniform packing of a polymer-based ion exchange resin with a bead size in the range of about 50 to about 250 μm. The mixing volume of the fluid fronts in the system of the invention is not more than 5% of the volume of the compartment.

REFERENCES:
patent: 5156736 (1992-10-01), Schoenrock
patent: 5565104 (1996-10-01), Priegnitz
patent: 5578216 (1996-11-01), Hotier et al.
patent: 5730877 (1998-03-01), Heikkila et al.
patent: 5755960 (1998-05-01), Callebert et al.
patent: 5770088 (1998-06-01), Ikeda et al.
patent: 6017448 (2000-01-01), Hotier et al.
patent: 6471861 (2002-10-01), Burgard et al.
patent: 2002/0011445 (2002-01-01), Lehoucq et al.
patent: WO 01/54790 (2001-08-01), None
Karl Schoenrock, “Performance Limits in Industrial Chromatographic Separation Processes*”,Zuckerind, vol. 122, No. 1, pp. 22-27, 1997.
Sergio Giacobello, et al., “Design of a Simulated Moving Bed Unit for Sucrose-Betaine Separations”,Journal of Chromatography A, vol. 872, pp. 23-35, ISSN 0021-9673, 2000.
Giovanni Biressi, et al., “Design and Optimisation of a Simulated Moving Bed Unit: Role of Deviations From Equilibrium Theory”,Journal of Chromatography A, vol. 876, pp. 3-15, 2000.

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