Separation of xylenes by extractive distillation

Distillation: processes – separatory – Adding material to distilland except water or steam per se – At least two materials

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203 56, 203 57, 203 60, 203 63, 203 65, 203 67, 585808, 585860, 585864, 585866, B01D 340, C07C 708

Patent

active

054416086

ABSTRACT:
p-Xylene cannot be separated from m-xylene by distillation or rectification because of the proximity of their boiling points. p-Xylene can be separated from m-xylene by means of extractive distillation. Effective agents are 3-ethylphenol and 1,1,2-trichloroethane. Effective agents for separating mixtures of p-xylene, m-xylene and o-xylene are 2-butoxyethyl acetate and 1,1,1-trichloroethane.

REFERENCES:
patent: 2494274 (1950-01-01), Woerner
patent: 2721170 (1955-10-01), Johnson
patent: 4673465 (1987-06-01), Berg et al.
patent: 5039380 (1991-08-01), Berg
patent: 5091059 (1992-02-01), Berg
patent: 5094723 (1992-03-01), Berg
patent: 5094725 (1992-03-01), Berg

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