Separation of propylene oxide from a mixture comprising...

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

Reexamination Certificate

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C549S538000, C203S053000, C203S054000, C203S057000, C203S058000

Reexamination Certificate

active

07323579

ABSTRACT:
A method of separating propylene oxide from a mixture (M) comprising 5 to 50 percent by weight propylene oxide and 50 to 85 percent by weight methanol, said method comprising(i) introducing said mixture (M) into an extractive distillation column;(ii) additionally introducing a polar solvent into said extractive distillation column;(iii) distilling propylene oxide overhead from said extractive distillation column at a bottoms temperature of from 40 to 70° C. and at a pressure of from 300 to 750 mbar.

REFERENCES:
patent: 4140588 (1979-02-01), Schmidt
patent: 5849938 (1998-12-01), Rueter et al.
patent: 6500311 (2002-12-01), Sawyer
patent: 118 873 (1976-03-01), None
patent: 0 811 617 (1997-12-01), None
patent: 1 424 332 (2004-06-01), None

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