Separation of methylene chloride from tetrahydrofuran by extract

Distillation: processes – separatory – Adding material to distilland except water or steam per se – Organic compound

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203 58, 203 60, 203 62, 203 63, 203 64, 549429, 570262, B01D 340, C07C 1738, C07D30708

Patent

active

054258545

ABSTRACT:
Methylene chloride is difficult to separate from tetrahydrofuran by conventional distillation or rectification because of the proximity of their vapor pressures. Methylene chloride can be readily separated from tetrahydrofuran by extractive distillation. Effective agents are 1-pentanol, 1,2-butanediol and 3-nitrotoluene.

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