Separation of isobutene non-reacted during polymerization of...

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Polymers from only ethylenic monomers or processes of...

Reexamination Certificate

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C526S348600, C526S348700, C526S071000

Reexamination Certificate

active

07105616

ABSTRACT:
A process for working up a liquid reaction discharge of the cationic polymerization of isobutene, which substantially comprises polyisobutene, unconverted isobutene and, if required, an inert diluent, is described. Problems with foam formation when the unconverted isobutene is being distilled off are avoided if the heated reaction discharge is let down into a flash container and/or not more than 900 m3/h of vapor are expelled per square meter of liquid surface and/or the resulting foam is destroyed, for example in a wet cyclone.

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Dr.-Ing Hermann Güterbock:“Polyisobutylen und Isobutylen-Mischpolymerisate”, Springer-Verlag, pp. 77-104 1959.

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