Separation of amine from a phenolic compound

Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing

Reexamination Certificate

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C564S439000

Reexamination Certificate

active

07049471

ABSTRACT:
A process comprises contacting a product mixture with a base, optionally in the presence of a polyhydric alcohol, to produce a base-treated mixture and distilling the base-treated mixture in which the product mixture comprises an aromatic amine and a phenolic compound.

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Ventor D L et al., Liquid-liquid equilibria for phenolic compounds, neutral oils, and nitrogen bases at 313.15 K, J. Chem Eng Data; Journal of Chemical and Engineering Data—Jul./Aug. 2001, vol. 46, No. 4, Jul. 2001, pp. 613-622, USA.
Yang, Guo-Hua et al., Simultaneous separation and concentration for phenol and aniline by distillation with added salts. Journal, Dept. of Chemical Engineering Univ. of Petroleum, Dongying, Shandong, 257061, Peop. Rep. China, Ranliao Huaxue Xuebao (2000), 28(4), 364-367.

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