Separation of active catalyst particles from spent catalyst part

Mineral oils: processes and products – Refining – Sulfur removal

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208 52CT, 208216R, 209 2, 209 20, 209138, 209471, 502 21, 502 26, 502 29, 502 30, 502 31, 502 34, 502 41, 502516, C10G 4508, B01J 3872, B01J 3856, B07B 700

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active

052098400

ABSTRACT:
Spent hydrotreating catalyst having carbonaceous and metallic deposits and of regular geometric shape after being stripped of process oil is fluidized by flowing air upwardly through the catalyst at a velocity sufficient to expand the bed thereby segregating the catalyst particles into a high activity, upper, less-contaminated fraction and a lower, more-contaminated fraction and recycling the high activity fraction to a hydrotreating process. Optionally, the high activity fraction can be regenerated with carbon burnoff or rejuvenated by acid leaching followed by regeneration with carbon burnoff to further improve catalyst activity.

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