Separation of 3-carene from limonene by extractive distillation

Distillation: processes – separatory – Adding material to distilland except water or steam per se – Organic compound

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203 59, 203 60, 203 62, 203 63, 203 64, 203 65, 203 67, 203 68, 203 69, 585860, 585864, 585866, 585867, B01D 340, C07C 708

Patent

active

058401601

ABSTRACT:
3-Carene is difficult to separate from limonene by conventional distillation or rectification because of the proximity of their boiling points. 3-Carene can be readily separated from limonene by extractive distillation. Effective agents are o-cresol, 2,6-dimethyl-4-heptanone and triethylene glycol.

REFERENCES:
patent: 4245075 (1981-01-01), Lepert
patent: 5084142 (1992-01-01), Berg et al.
patent: 5085739 (1992-02-01), Berg et al.
patent: 5380405 (1995-01-01), Berg
patent: 5582693 (1996-12-01), Berg
patent: 5597455 (1997-01-01), Berg

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