Separation of 3-carene and limonene by extractive distillation

Distillation: processes – separatory – Adding material to distilland except water or steam per se – Organic compound

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203 60, 203 63, 203 64, 203 65, 203 69, 585350, 585860, 585864, 585866, B01D 340, C07C 708

Patent

active

055974554

ABSTRACT:
3-Carene and limonene cannot be separated from each other by rectification because of the closeness of their boiling points. They are readily separated by extractive distillation. Effective agents are: diethylene glycol phenyl ether, nonyl phenol, tripropylene glycol methyl ether, ethyl salicylate, 4-ethylphenol and 2-phenoxyethanol.

REFERENCES:
patent: 2459433 (1949-01-01), Johnson et al.
patent: 3422029 (1969-01-01), Booth
patent: 5380405 (1995-01-01), Berg
patent: 5391264 (1995-02-01), Berg
patent: 5441608 (1995-08-01), Berg

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