Separation of 3-carene and limonene by azeotropic distillation

Distillation: processes – separatory – Adding material to distilland except water or steam per se – Organic compound

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203 58, 203 59, 203 60, 203 61, 203 62, 203 63, 203 64, 203 65, 203 68, 585350, 585860, 585865, 585866, B01D 336, C07C 706

Patent

active

055826938

ABSTRACT:
3-Carene and limonene cannot be separated from each other by rectification because of the closeness of their boiling points. They are readily separated by azeotropic distillation. Effective agents are: cyclopentanol, 2-nitropropane, ethyl formate amyl acetate dimethyl carbonate, tetrahydrofuran, acetic acid and 2-amino-amethyl-1-propanol.

REFERENCES:
patent: 2459433 (1949-01-01), Johnson et al.
patent: 5380405 (1995-01-01), Berg
patent: 5391264 (1995-02-01), Berg
patent: 5421965 (1995-06-01), Berg
patent: 5423955 (1995-06-01), Berg
patent: 5425853 (1995-06-01), Berg

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