Separation of 2-pentanol, 3-methyl-2-butanol and 1-butanol by az

Distillation: processes – separatory – Adding material to distilland except water or steam per se – Organic compound

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203 60, 203 62, 203 63, 203 64, 203 68, 203 69, 203 70, 568913, B01D 336, C07C 2982

Patent

active

054476089

ABSTRACT:
3-Methyl-2-butanol, 2-pentanol and 1-butanol are difficult to separate by conventional distillation or rectification because of the proximity of their boiling points. Mixtures of these three can be readily separated from each other by azeotropic distillation. Effective agents are hexyl acetate, hexane and 3-methyl pentane.

REFERENCES:
patent: 2483246 (1949-09-01), Stribley
patent: 2500329 (1950-03-01), Steitz
patent: 5338410 (1994-08-01), Berg

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