Separation of 2-methyl-1-butanol and 3-methyl-1-butanol from 1-p

Distillation: processes – separatory – Adding material to distilland except water or steam per se – Organic compound

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203 58, 203 59, 203 60, 203 62, 203 63, 203 64, 203 65, 203 68, 203 69, 203 70, 568913, B01D 340, C07C 2984

Patent

active

060248416

ABSTRACT:
2-Methyl-1-butanol and 3-methyl-1-butanol are difficult to separate from 1 pentanol by conventional distillation or rectification because of the proximity of their boiling points. 2-Methyl-1-butanol and 3-methyl-1-butanol can be easily separated from 1-pentanol by extractive distillation. Effective agents are 3-carene, propylene glycol phenyl ether and dimethylsulfoxide.

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patent: 5763695 (1998-06-01), Beg
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patent: 5789629 (1998-08-01), Berg

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