Separation and recovery of products obtained in catalytic proces

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Removing and recycling removed material from an ongoing...

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260 63N, 526 69, 526 82, 526341, 526342, 526328, 526330, 526347, 528503, C08F 440, C08F 600, C08F 2044

Patent

active

039650790

ABSTRACT:
Sulphur dioxide and unreacted monomer or mixture of monomers are separated and recovered from the polymer or copolymer slurry obtained by polymerizing acrylonitrile monomer or copolymerizing acrylonitrile monomer and a further ethylenically unsaturated monomer copolymerizable therewith in the presence of a catalytic system comprising sulphur dioxide or a sulphite, by a process comprising the steps of separately removing the sulphur dioxide and the monomer or mixture of monomers from the slurry in two distinct volatilization zones connected in series under decreasing subatmospheric pressures, scrubbing with water the sulphur dioxide vapors removed in the first zone and vapors of unreacted monomer or monomers removed in the second zone, and recycling the two resulting aqueous solutions to the polymerization or copolymerization medium.

REFERENCES:
patent: 3060159 (1962-10-01), Lea et al.
patent: 3454542 (1969-07-01), Cheape et al.

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