Separating toluene diisocyanate and/or higher boiling solvents f

Distillation: processes – separatory – Convective distillation with normally gaseous medium – e.g. – air

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203 88, 203 89, 203 90, B01D 310, C07C11904

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active

042895898

ABSTRACT:
A process for separating toluene diisocyanate and/or higher boiling solvents from distillation residues obtained from the phosgenation of toluene diamine in the presence of solvents wherein the separation takes place in a fluidized bed at temperatures of 140.degree. C. to 280.degree. C.

REFERENCES:
patent: 3457291 (1969-07-01), Baylor
patent: 3897314 (1975-07-01), Liebsch et al.
"Chemical Engineer's Handbook", Perry, 4th Ed., 1966, pp. 17-23 to 17-26, 20-50 to 20-54.

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