Self-diverting acid treatment with formic-acid-free...

Earth boring – well treating – and oil field chemistry – Preventing contaminant deposits in petroleum oil conduits

Reexamination Certificate

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C166S304000, C166S305100, C166S307000, C166S308100, C166S308200, C166S311000, C166S312000, C507S268000, C507S269000, C507S277000, C507S922000, C507S923000, C507S927000

Reexamination Certificate

active

07902124

ABSTRACT:
A method of treating a subterranean formation penetrated by a wellbore of a well having iron-containing components is carried out by introducing a treatment fluid into the wellbore of the well. The treatment fluid is formed from an aqueous solution, a mineral acid, a viscoelastic surfactant gelling agent and corrosion inhibitor system containing at least one of an alkyl, alkenyl, alicyclic or aromatic substituted aliphatic ketone and aliphatic or aromatic aldehyde. The treatment fluid is substantially free of any formic acid or precursor formic acid. In certain embodiments, the corrosion inhibitor system comprises a mixture of at least one of an alkenyl phenone or α,β-unsaturated aldehyde, an unsaturated ketone or unsaturated aldehyde other than the alkenyl phenone and α,β-unsaturated aldehyde, a dispersing agent, an extender and an alcohol solvent. A corrosion inhibitor intensifier may also be used in certain embodiments, which may include a mixture of cuprous iodide and cuprous chloride.

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SPE106185—Cassidy, J.M., McNeil, R.I., Kiser, C.E.—Understanding Formic Acid Decomposition as a Corrosion Inhibitor Intensifier in Strong Acid Environments. Feb. 28-Mar. 2, 2007, Society of Petroleum Engineers.
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