Sample injection timer for chromatographic apparatus

Measuring and testing – Sampler – sample handling – etc. – Analyzer supplier

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7386301, G01N 3012

Patent

active

047021152

ABSTRACT:
A method and apparatus for detecting the injection of a solvent borne sample into the injector port of a chromatograph having a carrier gas flow path for pressurizing the port. The gas pressure in a region adjacent the injector port is monitored. When vaporization of the solvent causes the carrier gas pressure to rise above the steady state value by a threshold amount, a control signal is generated which serves as an accurate time reference for the moment of sample injection into the injector port. The carrier gas pressure is monitored by time averaging the instantaneous carrier gas pressure and differentially sensing the instantaneous carrier gas pressure and the time averaged instantaneous carrier gas pressure. The time averaging is preferably done by flow restricting the carrier gas and accumulating the flow restricted carrier gas in a chamber.

REFERENCES:
patent: 3630088 (1971-12-01), Sawyer et al.
patent: 3649204 (1972-03-01), Farr
patent: 3668834 (1972-06-01), Deans
patent: 3800593 (1974-04-01), Bradley
patent: 3940994 (1976-03-01), Klee et al.
patent: 4035168 (1977-07-01), Jennings
patent: 4347215 (1982-08-01), Sisti et al.
patent: 4414857 (1983-11-01), Brazhnikov et al.
"Automatic Vapor Sampling for Gas Chromatographic Analysis"; Analytical Chemistry, vol. 38, No. 8, Jul. 1966, pp. 1097-1098; G. Szekely et al.

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