Sample holder for NMR measurements with field homogenization...

Electricity: measuring and testing – Particle precession resonance – Spectrometer components

Reexamination Certificate

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Reexamination Certificate

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07656158

ABSTRACT:
A sample vessel (80) made of material with magnetic susceptibility χ2, for containing a sample substance (87) with magnetic susceptibility χ3≠χ2to be analyzed in a nuclear magnetic resonance (NMR) spectrometer, has an inner interface G2toward the sample substance and an outer interface G1toward the environment (85) that exhibits magnetic susceptibility χ1. The shape of the interface toward the sample substance and the interface toward the environment are coordinated to match the discontinuities in susceptibility at the interfaces in such a way that on introduction of the sample tube filled with sample substance into the previously homogeneous magnetic field of an NMR spectrometer, the magnetic field inside the sample substance remains largely homogeneous.

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