Resistance-heated pyrolytic boron nitride coated graphite boat f

Electric heating – Heating devices – Resistive element: igniter type

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13 23, 13 25, 118726, 219427, 427 50, 427113, 4272481, 428408, 432265, H05B 312, F27B 2104, C23C 1312

Patent

active

042648033

ABSTRACT:
Resistance-heated vaporization boats for the vacuum vaporization of metals, such as aluminum, chromium, copper or the like, are made by machining a boat cavity in at least one side of a graphite bar. The bar is totally encapsulated over its entire outer surface, including the boat cavity, with a continuous coating of pyrolytic boron nitride (PBN). The PBN coating is removed from areas at both ends of the bar to provide electrical contact zones for connecting the bar to a power source. The sides and ends of the boat cavity have smooth contours without sharp corners and the ends of the cavity have a hemispherical configuration to resist longitudinal expansion of the PBN coating thereby preventing separation of the PBN coating from the surface of the graphite bar. The PBN coating is deposited from a gas at a temperature of 1750.degree. C. to 2300.degree. C. and has a thickness of at least 0.010 inch.

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