Replica film of specimen for electron microscopy apparatus

Plastic article or earthenware shaping or treating: apparatus – Shaping means employing anatomical body or portion thereof

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204165, 250311, 250326, 250441, 250442, 264 22, 264 28, 264 81, 264 83, 264222, 425174, 4251748E, 425289, 427 4, 427 39, 427 41, H05H 100

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043348440

ABSTRACT:
A uniform thin replica film of a specimen for electron microscopy having a high resolution power such as approximately 1 A is presented. This uniform thin replica film is directly prepared on the specimen by a plasma polymerization technique by depositing organic monomer vapors on a specimen placed on a negative electrode in a high vacuum atmosphere. The deposition is carried out by applying a discharge voltage of from 0.5 to 3 K.V.D.C. between a pair of positive and negative electrodes for 1 to 15 minutes to effect a glow discharge under the conditions of a current density of the glow discharge of from 0.1 and 2 mA/cm.sup.2 and a gas pressure of from 1 to 10.sup.-2 Torr in the system.

REFERENCES:
patent: 2875341 (1959-02-01), Nesh
patent: 3068510 (1962-12-01), Coleman
patent: 4012475 (1977-03-01), Kindel
patent: 4227080 (1980-10-01), Okura et al.
patent: 4242188 (1980-12-01), Niinomi et al.
"Styrene Resin Cracking Method for Observing Biological Materials by Scanning Electron Microscopy", Journal of Electron Microscopy, Tanaka et al., vol. 23, No. 4, pp. 313-315 (1974).

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