Removal of hydrogen sulfide

Chemistry of inorganic compounds – Modifying or removing component of normally gaseous mixture – Carbon dioxide or hydrogen sulfide component

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423222, 42324301, 42324401, 4235741, 423575, C01B 1716

Patent

active

053043618

ABSTRACT:
Improved processes are disclosed for the removal of hydrogen sulfide from feed streams by conversion of hydrogen sulfide and sulfur dioxide to elemental sulfur and water, e.g. Claus process. The feed stream of the present invention is divided into two split streams wherein one is incinerated to form sulfur dioxide in the presence of oxygen. The sulfur dioxide is then separated from the water, nitrogen and other impurities and combined with the other split stream to form a reactor feed which is passed to a sulfur reaction zone for conversion to elemental sulfur. Due to the rejection of water, nitrogen and other impurities from the reactor inlet stream, a higher concentration of hydrogen sulfide and sulfur dioxide can be achieved in the sulfur reaction zone. As a result, the processes of the present invention can be used to increase the throughput of existing Claus process plants and reduce the size of new Claus process plants.

REFERENCES:
patent: 3637352 (1972-01-01), Bratzler et al.
patent: 4085199 (1978-04-01), Singleton et al.
patent: 4113849 (1978-09-01), Atwood
patent: 4363791 (1982-12-01), Trentham et al.
patent: 4442083 (1984-04-01), Canales et al.
patent: 4450145 (1984-05-01), Klepeis
patent: 4988494 (1991-01-01), Lagas et al.
patent: 5019361 (1991-05-01), Hakka
"Look at Claus Unit Design" by D. Parnell Hydrocarbon Processing, Sep. 1985 pp. 114-118.
"Sulphur, Sulphur Dioxide and Sulphuric Acid" by U. H. F. Sander et al. 1984, The British Sulphur Coporation Ltd. pp. 42-90.
"High Recovery, lower emissions" by David K. Beavon et al. The Oil and Gas Journal, Mar. 12, 1979 pp. 76-80.
C. M. Yon, et al., "Integrated UCAP-A New Approach to Sulfur Recovery", 1979 NPRA Annual Meeting, Mar. 25-27, 1979.

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