Regeneration of polyborazylene

Details Regeneration of polyborazylene Regeneration of polyborazylene

2009-01-14

2010-12-07

Hendrickson, Stuart (Department: 1793)

Chemistry of inorganic compounds

Boron or compound thereof

Nitrogen and hydrogen containing

C252S188250, C252S188260, C423S284000, C423S658200

Reexamination Certificate

active

07846410

ABSTRACT:
Method of producing ammonia borane, comprising providing polyborazylene; digesting the polyborazylene with a dithiol-containing agent to produce a boro-sulfide compound and a byproduct; converting the byproduct to the boro-sulfide product of step (b) by reaction with a first alkyl-tin hydride; and, converting the boro-sulfide compound produced in steps (b) and (c) to ammonia borane by reaction with a second alkyl-tin hydride.

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