Reductive pyrolysis method for determining trace sulfur

Details Reductive pyrolysis method for determining trace sulfur Reductive pyrolysis method for determining trace sulfur

1980-09-30

1982-05-18

Schor, Kenneth M.

Chemistry: physical processes

Physical processes

Crystallization

204 1T, 422 80, G01N 2746

Patent

active

043302980

ABSTRACT:
Method for determining total organic sulfur using reductive pyrolysis and specific electrochemical detection of sulfide ion at a mercury electrode. The method is especially useful for the determination of sulfur in matrices containing halogen or nitrogen compounds. Under routine conditions, a detection limit of less than 50 parts per billion (ppb) can be achieved using differential pulse cathodic stripping voltammetry as the detection mode.

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