Reduction of nitroaromatic compounds

Details Reduction of nitroaromatic compounds Reduction of nitroaromatic compounds

1983-06-20

1984-10-30

Torrence, Dolph H.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07C12178

Patent

active

044799047

ABSTRACT:
Aminoarylacetonitriles, such as 2-(4-amino-3-fluorobenzene)propionitrile, are prepared by (1) isolating the crude reaction product from a process wherein a nitroaromatic compound has been reacted with an alpha,alpha-disubstituted acetonitrile in an inert solvent and in the presence of a base so as to form a nitroarylacetonitrile and (2) subjecting that crude reaction product to reduction in the presence of active iron powder and an aqueous alkanol.

REFERENCES:
patent: 4370278 (1983-01-01), Stahly et al.
March, Advanced Organic Chemistry (McGraw-Hill, New York, 1977), pp. 1125-1126.

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