Reduction furnace for quantitative deuterium determination in hy

Radiant energy – Ionic separation or analysis – With sample supply means

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73 2339, H01J 4904

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06046450&

ABSTRACT:
The invention relates to a method for the quantitative determination of deuterium in samples containing hydrogen, and to a reduction oven for reducing gaseous or liquid substances containing hydrogen, which may be coupled directly to an isotope ratio mass spectrometer (IRMS), thereby permitting an online-coupled, reliable deuterium determination which can be automatized.

REFERENCES:
patent: 4332591 (1982-06-01), Oi
patent: 4916313 (1990-04-01), Hall
patent: 5432344 (1995-07-01), Brand
patent: 5976890 (1999-11-01), Gehre et al.
A.D. Morse et al.,; An Investigation into the Cause of Memory Effects Associated with the Conversion of H.sub.2 O to H.sub.2 for D/H Measurement; Chemical Geology (Isotope Geoscience Section), 107 (1993) pp. 147-158.
I.S. Begley et al.; On-line Reduction of H.sub.2 O for o.sup.2 H and o.sup.18 O Measurement by Continuous-flow Isotope Ratio Mass Spectrometry; Rapid Communications in Mass Spectrometry, vol. 10, 1996 pp. 969-973.

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