Reducing the monomer content in expandable thermoplastic beads

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Cellular products or processes of preparing a cellular...

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526 80, C08J 920

Patent

active

041478452

ABSTRACT:
The invention relates to a process for reducing the monomer content in expandable thermoplastic beads which are produced by polymerizing an ethylenically unsaturated monomer or a mixture of such monomers in aqueous suspension in the presence of a blowing agent. The residual monomers in both the beads and the process water are reduced by treatment of the slurry of beads and water obtained after polymerization in a vessel at a temperature above 65.degree. C. in the presence of at least one water-soluble initiator. In order to avoid the expansion of the beads during the course of monomer reduction the vessel is kept completely filled with a liquid, preferably water, during the temperature treatment.

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